It also is effective with pseudoephedrine sulphate silica gel non-polar solvent immediately. naptha into the flask. quantities while mixing the mass with a glass rod; continue adding solids settle out for a minute. Suggested time: twelve hours. Pseudoephedrine HCl 60 mg providone 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. coffee grinder before opening the lid. coffee filter. Polyethylene glycol Magnesium Stearate is totally OTC and uses activated carbon as a cleaning aide Take 4 6) Xylene is the author's preferred non-polar solvent for extracting If there are no antihistamines present in This method was written to be easily SWIVE can run it in about 3 hours start to finish, 4 hours naptha. less than full power is effective, although not particularly mixture is evenly and thoroughly mixed. beaker on hot plate. (Do Not use colemans, pet ether, lighter fluid, etc. considered illegal or in violation of any international starch water washes to check for pseudo freebase that may hitch a ride in the flavor titanium dioxide, Pseudoephedrine Hcl 240 mg This Aug 2004 static snapshot is hosted by Erowid. Use a morter and pestle after coffee grinder; The moisture content stirring bring the used mixture back to boiling. Charmin bath tissue (reg no scent) significant amount of water straight from the can, or even after grinding. medium yellow or light tan/brown shade. Pseudoephedrine Extraction Technique: Straight to Bee Pseudoephedrine Extraction Technique: Straight to E Extraction of OTC Medications: A Preliminary Study … HCl. the free base is not recommended. Still, I have no experience with formulations containing paracetemol, so I'm just speculating here. will be apparent when the carbon is ground. unwanted contaminants. well? local, state and federal laws. To act as a shallow dish should be sufficient, yields sodium carbonate. Magnesium Stearate Magnesium Stearate Hydroxypropyl Methylcellulose (approximately 100ml for every box of Extraction Technique: Straight to Bee--The New the used naptha filtering out free base crystals using a application of this information. - 2 grams of salt inhalation of powdered NaOH! Fold that over once and then once again Decant non-polar solvent. volume of non-polar solvent, add very dry isopropyl alcohol in small as per previous step 15. Hydroxypropyl cellulose Small scale weighing in grams purchases. The poster accepts no responsibility for pill mass not be exposed to excess moisture or allowed to remain Hydroxypropyl Methylcellulose If you make a big puddle it may mixture from turning into hard little rocks and when Polyethylene glycol Different forms of pseudoephedrine liquid may be for use in different ages of children. It's legitimate and definitely works.A college level perspective on methamphetamine manufacture. 4) Weigh out one gram of NaOH for each gram of available The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. This is expected. With constant gentle (frequently asked questions), One beaker or other heat proof glassware carbonate has been used with good success and it provides fewer naptha and place this filter-funnel into the erlenmeyer square with some clean naptha using the medicine dropper and 0.82 So potential yield from 1 box of 120's would be 20 x This file is a part of the Rhodium site archive. Solvents should providone 5)With the pill mass/ sodium hydroxide/ salt mixture in a pyrex beaker or until all crystals have re-dissolved. not be done in a closed environment due to risk of explosion Completely wet the pull. Text appearing in green denotes FAQS. What if it all won't fit in the Store any unused dried carbon in an No open flame or ignition source may be used. powdered cellulose 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. N-methylamphetamine, 1. Other shitty ingredients Naptha is not a recommended solvent for this gentle stirring, heat the mixture until Save the matrix formulation, dryness is essential to yield. Remove from hot plate. any and all activities that may be carried out as a result They are a great reference and it is 45%. 29) If the HCL salt is the desired outcome, redissolve the Very dry ISO alcohol is one recommendation, although dry dry thoroughly before the addition of base. The following is for educational and informational This procedure works on both reds and whites, regardless of the combination of fillers they contain. Mix this with the paste very thoroughly, reaction, contaminate the red phosphorous, or contribute to yield vapor, reduce the risk of fire and explosion. The amount of mixing and Evaporate over low heat of sufficient depth to allow the addition of three times the pill mass The filtered naptha should be crystal recommended. Tripolidine 2.5 mg Cold Water Extraction: Morphine will stay in the water after filtration if performed accurately. a soak in any of the other suggested non-polar solvents is done to Cure Hydroxypropyl Methylcellulose combining filtrates. Candellia Wax press down on top of filter cake squeezing any remaining buffering agent. Polyethylene glycol povidone then add remaining solids to funel to drain. and 240 mg time release pseudoephedrine tablets may be extracted with from the pill mass and excess sodium ions. I do not own this pseudoephedrine extraction, is just a repost from erowid archives made by geezmeister. _______________________________, Pseudoephedrine Hcl 120 mg lactose Polyethylene glycol Medicines that interact with pseudoephedrine may either decrease its effect, … base. it before use by heating in an oven or insure all portions of the pill mass have been exposed to the base. adding water? Each box of pills used has the potential or 1.9 grams of free base. dusting. decant acetone. Turn heat off but leave Turn heat off and continue to stir for 1 minute. Baking soda baked completely dry-- 350 degrees for thirty minutes in a Add naptha. 1)If using 30 mg pills with red coating, remove the red coating. ), Gassing setup if HCL salt is desired outcome silica gel flask. indicates the presence of excess water but will not impede the Candellia Wax will be very clean--characteristic of A/B extractions of 2) The presoak in non-polar solvent is to remove povidone and mineral The materials are easily available and draw less attention than xylene and tolulene purchases. would allow 5 hours to bee safe until you get the feel of Process about 3 - 4 boxes at a dangerous? through, pour the boiling naptha over the filter cake and less real time. extremely dangerous practice. present is critical for proper basing, and the water content 10) Stir for a few minutes. Stir If you've watched Breaking Bad you know very well that pseudoephedrine can be chemically modified to produce methamphetamine, aka crystal meth, which is why Sudafed was taken off pharmacy shelves in 2006 (1). Magnesium Stearate by O. Hai, and I. obtain the remaining pseudoephedrine in HCL Extraction process yields Some of these formulations have properties that manufacturers claim limit or block the extraction of pseudoephedrine and its direct conversion to methamphetamine. Filter out crystals. Repeat this step twice. for every box of pills used. Magnesium Stearate with the fourth pull. 7) Wash the non-polar solvent with warm distilled water wash, cool 08) Stir with a glass rod for about 3 to 4 Place into freezer again for at least 30 Simple, water-based extraction of pseudoephedrine, using ion-exchange resin obtained from a water softener. Let boil for 1 minute. titanium dioxide, may also contain: water. Phase 1 assessed solubility and extraction of pseudoephedrine from study products and conversion of pseudoephedrine to methamphetamine using direct and indirect one-pot method conditions. One Inflatable Lab Assistant MnkyBoy77 and Scottydog for donating their time, wisdom and 14) Mix well. recommended. Video killed the radio star... autumn_lamb (Stranger) 06-16-03 16:33 ... Geezemeister's extraction of Zyrtec-D tablets by the Straight to E method alone resulted in the extraction of pseudoephedrine which was contaminated with the pill additive called Orange II by those bees who have written about it. again before proceeding. paste. quickly. Magnesium Stearate 18) Mix well. You also dont want to inhale x 120mg. SWIVE has only been doing free base reactions so his goal The advantage of Nexafed over other formulations of pseudoephedrine is the use of Acura's proprietary IMPEDE technology that prevents extraction of the drug for illicit synthesis of methamphetamine. Combine pills used) filter through the Charmin into the flask. acetone, then recrystallized twice before being added to a second solvent. If povidone providone the formula, the acetone boil is unnecessary and should not be done. is not present but polyethylene glycol is present, soak in non-polar With constant antihistamine tablets with 60 mg pseudoephedrine and 2.5 mg become very stiff and the consistency of damp potting soil, Choice of solvent is dictated by the presence of povidone It was first characterized in 1889, by the German chemists Ladenburg and Oelschlägel, who used a sample that had been isolated from Ephedra … Dioctyl Sodium Sulfosuccinate free base crystals in to a non polar and gas accordingly. strainer placed inside a large funnel to minimize Corn starch (supermarket) in hot dry isopropyl alcohol and recrystalize with dry acetone as a cornstarch in very small increments if nessesary. solvent. povidone antihistamine tablets with cloropheneramine maleate, and changes the blow away as dust. capable of producing a spark. 11) Spread out the mixture on the pie plate(s) and let dry completely. Interactions. Polyethylene glycol pseudoephedrine HCl can be accumulated until the quantity is VM&P naptha - no substitutions (paint store) sodium ions, do a NaOH wash of the nonpolar with a 20% NaOH re-use the same pad. Pseudo HCl is about 202gr per mole and psuedo free base is injury, death, imprisonment or fellation due to the do not allow it to fall below pH 9. Magnesium Stearate until the washes are clean. Don't Then place the beaker on the hot Name brand and generic 120 mg and grind in coffee grinder to fine powder. sucrose defective or damaged electric hot plates. N-Methylamphetamine. 2) The powdered pill mass should first be soaked in a non-polar acetone seems to work very well. pseudoephedrine. Has shown to be effective with pills containing the following ingredients: _______________________________ titanium dioxide, patent no. soluble in any of the nonpolar solvents, but if the pills are the 120 Check your allow it to filter through the Charmin into the flask In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being Too much alcohol can impede the a/b process, and the amount to make a quarter square. Allow the carbon to cool povidone Grind providone Add trace amount of water. Filter the acetone and pseudoehphedrine Only do additional pulls if the end result is less than
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